Abstract
Present study describes a simultaneous and highly reproducible, large-scale, one-pot, template free synthesis of nearly homogeneous and blue luminescent CdSe nanoparticles (NPs) in a single reaction at 50°C by wet chemical method. The method is simple, inexpensive and ensures almost complete utilization of the precursors. The product was well characterized by X-ray diffraction, UV-Vis. spectroscopy, Fourier transform infrared spectroscopy and Transmission electron microscopy. X-ray diffraction pattern indicates that CdSe NPs possess a Wurtzite (Hexagonal) structure. Systematic particle size dependent ‘blue shift’ is observed in optical absorption edge. Transmission electron microscopy showed that the particles diameters are in the range of 5 – 8 nm.
Keywords: Blue shift, FTIR spectroscopy, semiconductor nanoparticles, transmission electron microscopy, UV-Vis spectroscopy, Wurtzite structure
Current Nanoscience
Title: Synthesis of CdSe Nanoparticles at 50°C by Wet Chemical Method
Volume: 6 Issue: 1
Author(s): Pushpendra Kumar and Kedar Singh
Affiliation:
Keywords: Blue shift, FTIR spectroscopy, semiconductor nanoparticles, transmission electron microscopy, UV-Vis spectroscopy, Wurtzite structure
Abstract: Present study describes a simultaneous and highly reproducible, large-scale, one-pot, template free synthesis of nearly homogeneous and blue luminescent CdSe nanoparticles (NPs) in a single reaction at 50°C by wet chemical method. The method is simple, inexpensive and ensures almost complete utilization of the precursors. The product was well characterized by X-ray diffraction, UV-Vis. spectroscopy, Fourier transform infrared spectroscopy and Transmission electron microscopy. X-ray diffraction pattern indicates that CdSe NPs possess a Wurtzite (Hexagonal) structure. Systematic particle size dependent ‘blue shift’ is observed in optical absorption edge. Transmission electron microscopy showed that the particles diameters are in the range of 5 – 8 nm.
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Cite this article as:
Kumar Pushpendra and Singh Kedar, Synthesis of CdSe Nanoparticles at 50°C by Wet Chemical Method, Current Nanoscience 2010; 6 (1) . https://dx.doi.org/10.2174/157341310790226333
DOI https://dx.doi.org/10.2174/157341310790226333 |
Print ISSN 1573-4137 |
Publisher Name Bentham Science Publisher |
Online ISSN 1875-6786 |
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