Abstract
Several monosaccharides were peracetylated in excellent isolated yields (89-100%) with vinyl acetate in aqueous Na3PO4. The per-O-acetylation reaction is fast and mild, as well as insensitive to water. Meanwhile, the workup is convenient and the catalyst can be recycled easily.
Keywords: Acetylation, monosaccharide, vinyl acetate, catalyst, sodium phosphate
Letters in Organic Chemistry
Title: Convenient Per-O-Acetylation of Monosaccharides with Vinyl Acetate/ Na3PO4-H2O
Volume: 3 Issue: 12
Author(s): Chun-juan Shi, Jianbo Zhang, Jie Fu and Jie Tang
Affiliation:
Keywords: Acetylation, monosaccharide, vinyl acetate, catalyst, sodium phosphate
Abstract: Several monosaccharides were peracetylated in excellent isolated yields (89-100%) with vinyl acetate in aqueous Na3PO4. The per-O-acetylation reaction is fast and mild, as well as insensitive to water. Meanwhile, the workup is convenient and the catalyst can be recycled easily.
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Cite this article as:
Shi Chun-juan, Zhang Jianbo, Fu Jie and Tang Jie, Convenient Per-O-Acetylation of Monosaccharides with Vinyl Acetate/ Na3PO4-H2O, Letters in Organic Chemistry 2006; 3 (12) . https://dx.doi.org/10.2174/157017806779468013
DOI https://dx.doi.org/10.2174/157017806779468013 |
Print ISSN 1570-1786 |
Publisher Name Bentham Science Publisher |
Online ISSN 1875-6255 |
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